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ILLUMINATI PSYCHE TWO STATION 2 -STORY SCROLL SITE
-AND-
-WEBSITE CONGLOMERATION PATH REPORTING--
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DISCLAIMER--
IDEAS ISSUES IF

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PATH ELECTRIC AND ELECRTROMAGNET STORY ROUTE WITH PATH STORIES OF ROUTE NOTES

COPPER IN PATH OF NUCLEAR GAS STORIES ROUTE NOTES

PATH ELECTRIC 2 DIRECTION UNDERWATER ROUTE STORIES NOTES

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FOREVER ABSTRACT ISSUE TO FOOD TO SPACE TO BACKWARDS STORIES ROUTE WITH LIFE ISSUE TO FOREVER STORIES NOTES

PATH WITH STEM CELLS AND CELLS STORY ROUTE WITH TOPIC OF MUTATIONAL STEM CELLS NUCLEAR NANO AND BRIDGE SALT STAGNENT STEM CELLS TOPICS WITH LIFE STORIES OF ICE STORIES TOPICS OF PASSAGE ROUTE NOTES STORIES OF DREAMS OF FROZEN IN GREEN VAPOR STORIES

 

THIS STOYR OF PATH TOPIC OF GREEN VAPOR TO ROUTE ICE STORIES OF EFFECT MEMORY ROUTE WITH LIFE STORIES

TOPIC IN MAX TRANSPORTATION STORIES NOTES PATH NOTES

TO STORIES OF ROUTE WORKING CONCUBIND STORIES OF DOT ICE ALSO ROUTE WITH STORIES

 

AND THAT STORY OF TOPIC ROUTE WITH STORY OF ROUTE GREEN VAPOR STORY IN ROUTE OF ISSUE PATH NUCLEAR GAS STORY PATH WITH TOPICS ROUTE WITH WORK WITH STORIES OF EFFECT WEATHER STORIES ROUTE WITH PATH

IN HISTORY WORKED TAR WOOD STORIES ALSO 

AND THE STORY OF TOPIC OF SMOKE NUCLEAR GAS WAS IN STORIES HISTORY ROUTE OF REJUVINATE BATTERY STORIES NOTES

TO THEN MAKE ELECTRIC NOTES STORIES NOTES

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TO GREEN VAPOR STORIES NOTES PATH WITH NOTES

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TOPICS OF EFFECTED BY STORIES OF TOPIC ELECTRIC 2 DIFFERENT DIRECTIONS STORY UNDERWATER TO REACH STORIES OF PATH ROUTE OF CYROGENIC STORY OF PATH WITH VINEGAR BAKING SODA OF METHODIC EVENT OF BALL SPRING PRESSURE CANNISTER STORY ROUTE WITH PATH STORIES OF ISSUE TOPIC OF PATH VORTEX CANNON ROUTE OF PATH WORK ROUTE OF TUBE IN AND TUBE OUT STORIES OF CANNISTER ROUTE OF STORY TOPIC

ALSO NOTE STORIES OF ROUTE TOPICS OF TUBE OUT RIGHT AWAY STORY IN TIME NOTES WORK 2 DIRECTIONS

IN BACKWARDS STORY ROUTE WITH GREEN VX GAS IN THIS ROUTE PREFIX SUFFIX ISSUE STORIES NOTES OF DROPPING DOWN OUT OF CANNISTER RIGHT AWAY NOTES

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PATH EFFECT WEATHER AND EARTHQUAKES ROUTE STORIES NOTES

PATH OF ROUTE USE THE HISTORY OF COPPER 27 DOUBLE LEVERAGE ROUTE OF STORY ISSUE PATH OF BATTERY AND ELECTRIC

INTO 2 DIRECTIONS UNDERWATER ROUTE STORIES PATH WITH TOPICS 

TO STORIES

SIDE NOTE IN PATH OF STORIES OF ISSUE TOPICS OF NOTES

CANNISTER TOPICS WITH VX GAS VORTEX CANNISTER PATH WITH NOTES PREFIX SUFFIX ISSUE NOTES

TO STORY OF 2 DIRECTION UNDERWATER ROUTE TO CYROGENIC CHAMBER STORY TOPIC

WITH ELECTRIC ELECTROMAGNET

ELECTRON PROTON BASHING DOUBLE

AND PATH WITH TELSA COIL ROUTE WITH STORIES

IN COIL AND 27 COPPER COIL ROUTE TOPICS OF COIL ELECTRIC ELECTRO MAGNET PATH WITH STORIES

TO WONDERS ADD STORY OF COPPER ELECTRO ELECTRO MAGNET

OF BATTERY STORY UNDERWATER TOPIC OF THAT STORY ISSUE

ROUTE OF 2 DIRECTION STORY ROUTE WITH PERHAPS A STORY

OF NOT AN ELECTRIC STORY GET INTO THE TERM COMPLETE IN LIFE ATTITUDE WITH THIS PATH OF ROUTE STORIES

IN TOPIC

ADDING ELECTRIC ELECTROMAGNET TO COPPER COIL

AND ISSUE IN ROUTE OF TELSA COIL AREA AND TIN DISSOLVE AND ROUTE WITH PATH ELECTRON PROTON BASHING ROUTE

STORIES OF ELEMENTS IN THIS PATH OF STORIES 

IN TOPICS OF DOT AND SPHERE STORIES ROUTE NOTES

PATH NOTES

DOT BASHING STORY ELECTRON PROTON

AND TELSA COIL STORY OF SPHERE STORIES ROUTE WITH STORIES OF PATH NOTES ELECTRIC ELECTROMAGNET NOTES

IN POWER ANCHOR STORIES COMPLETE STORIES BEGIN TO WORK

 

SO THE STORY OF TOPIC OF ISSUE GREEN VAPOR STORY

IN NUCLEAR GAS WORK THIS STORY ROUTE WITH NOTES

 

TO STORIES OF WHY BATTERY UNDERWATER TOPIC IN POWER ANCHOR STORIES NOTES 

AND COMPLETE IN STORIES ADDING ELECTRIC ELECTROMAGNET TO COPPER ROUTE 

 

WAS A HISTORY OF MURITIC ACID 6 MOTIONS STORY

NOW IN 6 HEIGHT GAS PATH TO USE THAT STORY IN ROUTE WORKING WITH POWER NUCLEAR ROUTE WITH SMOKE PRESSURE

SPIN STORIES NOTES

 

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ISSUE TO NOTES PATH OF TOPIC OF STORY OF DOUBLE LEVERAGE COIL COPPER ROUTE WITH STORIES OF TOPICS OF ISSUE TO STORIES OF NOTES THE VARIATION OF THAT AND A COIL ROUTE WITH PATH ELECTRIC AND ELECTROMAGNET PATH STORIES OF EFFECTED BY THE ROUTE OF 2 DIRECTIONAL BATTERY UNDERWATER ROUTE WITH TOPIC OF EFFECT TIN DISSOLVE UNDERWATER ROUTE PATH WITH STORIES OF ROUTE THROUGH THAT PATH ROUTE STORIES INTO A CHAMBER OF ISSUE STORIES OF PRESSURE TO NOTE STORIES OF CYROGENIC STORY OF COLD EFFECT METHODIC EFFECTED STORY OF BALL SPRING TO BUBBLES ROUTE STORIES TO BOTH COLD MATTER VARIABLES AND METHODIC STORY ROUTE TO CYROGENIC STORY NOTES TO TOPIC OF BATTERY VARIANCE ELECTRIC ISSUE STORY ROUTE WITH DOUBLE LEVERAGE COPPER ROUTE STORIES OF TOPIC PLANE TO COIL ROUTE EFFECTED IN 27 COPPER COILS TOPIC ROUTE OF PATH NUCLEAR VAPOR STORIES THAT ONCE WORKED STORY OF ROUTE NOTES TOPIC OF SHAKE ISSUE GREEN NUCLEAR X PREFIX SUFFIX ISSUE DRAW TO STORY OF ROUTE TOPIC OF ISSUE STORIES NOTES OF TURBINE DISK SPIN GAP TUBE STORIES NOTES TOPICS

 

SO THE STORY OF 6 HEIGHT GAS ROUTE TOPIC REACHED THE STORY OF PATH WAS A HISTORY OF COPPER COIL DOUBLE LEVERAGE STORY OF TOPIC OF ISSUE STORY OF ISSUE BATTERY VARIANCE ELECTRIC STORY TOPIC OF BOTHERS TOPIC OF LIFE IN MURITIC ACID 6 MOTIONS STORY IN LIFE 3 BACKWARDS AND 3 FORWARD STORIES NOTES TOPICS NOTES

WHICH WAS ONCE THE STORY OF ROUTE TOPICS OF PATH STORIES NOTES 6 MURITIC ACID MOTIONS

NOW IN 6  HEIGHT GAS HISTORY ROUTE LEMON AND LIME NOTES

 

THAT STORY OF TOPIC ROUTE STORIES WENT TO STORIES OF PATH NOTES

ISSUE TO PATH 

 

THE STORY OF GREEN VAPOR ROUTE WENT TO STORIES LIGHTENING TURNED GREEN NOTES EVENT PATH OF WORKING WITH 2 DIRECTION OF ELECTRICITY UNDERWATER PATH TO BEGIN WITH NOTES

OF TOPIC OF NOTES HYDROGEN SULFIDE METAL TOPICS NOTES PATH INTO BRIDGE SALT STORIES ROUTE TO TOPIC OF STORIES PERHAPS THE STORY OF ICE STORY ROUTE WITH CLONES REACHED A STORY OF LIFE WITH TOPIC OF STORIES OF LIFE WITH CONCUBIND STORY ROUTE WITH LIFE NOTES AND PERHAPS THE TERM COMPLETE IN LIFE STORIES ROUTE WITH TOPICS BEGIN STORIES NOTES

 

THE ROOM OF THE PATH OF STORIES OF TOPIC OF 6 HEIGHT GAS STORIES OF LEMON AND LIME PATH TOPICS OF PRESSURE NOTES STORIES

SO THE PATH OF GAS REACHED LEVELS OF LEMON TO ALCOHOL BEFORE SALT

AND PATH WITH STORIES OF TOPICS ROUTE I PREFIX SUFFIX ISSUE HEIGHT TWICE STORY ROUTE WITH GREEN MATCHES STORY

ROUTE WITH TOPICS TO ACETONE ROUTE WITH STORIES TO PATH OF ROUTE WITH NOTES LIME MOLD ROUTE WITH STORIES

PATH NOTES IN STORIES OF METHYL ALCOHOL ROUTE WITH STORIES OF PATH WITH NOTES ISSUE STORY TO NOTES TOPIC

STORIES ROUTE WITH NOTES PATH NOTES BLUE LUBE AND RED LUBE STORIES NOTES TOPICS PATH NOTES

 

THE STORY OF FORMALDEHYDE WENT TO STORIES OF PATH LYE FLOWERS 5 TO 6 STORY ROUTE OF 

PATH DANDELION AND SUNFLOWER AND PATH WITH NOTES WHITE AND PURPLE FLOWERS AND PATH WITH CHAMOMILE STORY ROUTE WITH NOTES

AND PATH WITH NOTES LAVENDER ROUTE TOPICS WONDERS PERHAPS

THE VARAIBLES OF LYE TO FLOWERS TO WORK STORY OF PRESSURE

NAMES OF THE FLOWERS TOPIC TO ACTUALLY THAT PRESSURE OF THE FLOWERS TO WORK WITH TOPICS

ROUTE WITH STORIES

 

TO STORIES WORKED THE TOPIC OF UV ROUTE PREFIX SUFFIX ISSUES WITH STORIES CHAMOMILE ROUTE WITH FORMALDEHYDE 27 1 SALT PATH ROUTE

TO STORIES OF TOPIC NOTES ISSUE ROUTE WITH NOTES UV PREFIX SUFFIX ISSUES AND WHITE ROUTE WORK UV ISSUE STORY ROUTE WITH TOPICS

OF PATH WITH LIFE STORIES OF ISSUE TO NOTES THIS PASSAGE SKIPPING  THE SUNFLOWER BOUND TO THE FORMALDEHYDE AND

PATH WITH NOTES STORIES WITH THE ROUTE OF THE TOPIC OF BOUND AGAIN IN TOPIC

WONDERS

IN WORKING PURITY WITH UV STORIES ROUTE WITH AND WORKING STORY OF ANHYDROUS AMMONIA ROUTE WITH PATH NOTES

POTATO WHITE GLUE VINEGAR AND AMMONIA AND GOO AMMONIA TOPIC ROUTE WITH STORIES WONDERS

NOTE LYSOL PRODUCT NOTES TO PATH WORK POWER ROUTE STORIES TOPICS ROUTE WITH TOPICS OF LYE MURITIC ACID TO STORIES

OF POTATO AND DIRT AND SALT STORIES TOPIC TO ADD DIRT TO THIS PATH WITH STORIES NOTES

AND WORK WITH ANCHOR ROUTE WITH TOPICS OF LIFE WITH DIRT VARIABLES OF TOPICS WITH POWER STORIES AND THAT WORK WITH PATH OF ROUTE STORIES NOTES ISSUE TO NOTES PATH NOTES TO ANCHOR POWER AND ANCHOR ISSUE OF PATH ROUTE NOTES ISSUE TO ANHDYDROUS AMMONIA EFFECT PATH WITH STORIES OF CHOOSE A STORY NOTES

TO THE TOPIC OF ROUTE ISSUE

WORK WITH ANCHOR STORIES TO POWER ROUTE WITH TOPICS BEGIN ROUTE WITH NOTES STORIES NOTES

 

TO STORY OF THAT ROOM TO WORK STORIES OF TUBE RISE STORY WITH PATH LIGHTENING PRESSURE MACHINE AND EARTHQUAKES NOTES

IN TOPIC OF THAT TUBE ROUTE WITH STORIES OF TRIANGLE AND CUBE STORIES OF PATH WITH LIGHTENING STORY LINK WITH ROUTE IN STORIES

 

OF TOPICS OF 3 COIL TO TUBE ROUTE WITH STORIES OF PATH TRIPLE DENSE AND TRIPLE MOTOIN STORY NOTES

AND PATH WITH STORIES OF ROUTE WITH TURBINE DISK SPIN STORIES ALSO NOTES 

 

TO WORK A STORY OF ROUTE NOTES

THIS MACHINE WORK WITH UNDERGROUND TOPICS NOTES

 

IN VARIANCE TO UNDERWATER STORIES ROOM TO PATH TOPIC STORIES

 

TO PATH WITH GIANT BODY TOPICS ROUTE WITH STORIES OF ROUTE TOPICS ISSUE TO NOTES STORIES

OF PATH NOTES

 

OF RESEARCH PROJECT ROUTE WITH LIFE STORIES OF TOPIC OF ISSUE ROUTE

WITH A 4 STORY OF GOAL CHANGE GOAL AND WORKER AND CHOOSE WORKER ISSUE STORY

WITH DOUBLE BLACK AND WHITE STORIES OF THAT VARIABLE NOTES

 

TO STORY OF ROUTE WITH NOTES STORIES OF ISSUE

THAT STORY ROUTE WITH TOPIC THE PRESSURE OF GIANT BODY STORIES ISSUE NOTES

TO THE VARIABLE OF HOUSING STORY OF SILICONE NITROGEN METAL

TO VARIABLES

 

OF STORY HYDROGEN SULFIDE AND PATH WITH LIGHTENING

AND PATH WITH NOTES

 

TO STORY OF TOPIC OF 5 ANTENNA STORY OF ISSUE ROUTE WITH PROPYELENE GLYCOL OF PRESSURE TOPIC

OUTLINE SIDES WORK WITIH SPIN ELECTRIC TWICE IN CUBE STORY TOPIC ISSUE ROUTE

TO STORIES OF ISSUE JUST DO ONCE WITH ISSUE IN ROUTE SPIN COPPER MAGNET STORIES NOTES

ELECTRIC TOPIC IN CUBE IN STORIES

OF WHAT IS THE DIFFERENCE IN CUBE PRESSURE TO THAT STORY

ROUTE WITH STORIES OF LIFE WITH NOTES CUBE STORY OF TOBACCO ROUTE OF OUTLINE SIDES STORY OF TOBACCO

AND PUT POLE IN MIDDLE LEVERAGE ISSUE TO VARIANCE OF ISSUE TO JUST CONNECT STORIES

 

THESE TOPICS IN LIFE REACH STOREIS IN LIFE ISSUE TO WOMEN IN LIFE STORIES ROUTE WITH LIFE NOTES ISSUE

TOPICS WITH LIFE NOTES PATH WITH T BAR STORIES ROUTE OF HALF TUBE UNDERGROUND AND HALF ABOVE GROUND STORIES

VARIANCE T BAR STORIES WORK WITH STORIES OF 2 T BAR ROUTE CONNECT TO EACH OTHER STORY OF TOPIC PREFIX SUFFIX ISSUE

OF STORY ROUTE WITH NOTES THAT TOPIC IN DOUBLE LEVERAGE NOTE STORIES NOTES PATH WITH STORIES

OF PERHAPS TUBE UNDERWATER BRIDGE ON STORY WORK WITH T BAR ISSUE PREFIX SUFFIX ISSUES STORY

OF PATH WITH 

 

STORIES NOTES ALSO REACHES STORY OF PRESSURE WOMEN IN LIFE TO STRUCTURE WORK WITH MOVIES STORY PERHAPS A STORY

OF GET OUT OF STORY IN LIFE WONDERS ISSUE TO STORIES GET BACK INTO STORIES OF LIFE WITH NOTES

TOPICS WITH LIFE STORIES OF MAKING STUFF NOTES

 

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PERHAPS TO WORK 

 

THE STORY OF ROUTE ISSUE TO TOPIC

OF TARGET LIGHTENING WITH CUBE VARIABLES UNDERGROUND TO TRIANGLE STORIES ROUTE WITH STORIES

TO HAVE TO WORK THAT ROUTE TRIANGLE TO CUBE CONSTANT STORIES DOES NOT SEPERATE 2 ISSUE STORY 

TO STAY WITH

 

FLURRY AND FUZZY ROUTE WITH TOPICS OF OPIATE ROUTE WITH STORIES OF ISSUE ROUTE ONE ROUND OF ATTACK

EXTRA PLANE 911 STORY ROUTE WITH TOPICS

OF WORKING DIGNITY AND EGO STORIES OF LIFE ISSUE STORIES NOTES

 

TO TOPIC OF ISSUE TO THE EFFECT OF IMPLICATION OF ISSUE STORY TO BE A VARIABLE IN LIFE OF UNDERWATER TO TUBE TO BRIDGE

STORY ROUTE WITH PATH DOUBLE GRAVITY VALUE PLANET AND PATH WITH SUN STORIES TOPICS TO TANGENT SPHERE TO BODY

STORIES ROUTE WITH LIFE NOTES

 

THE TOPIC OF CLOSED OFF TUBE ROUTE WITH STORIES OF DIRECTIONAL STORIES ROUTE WITH LIFE NOTES

TO PERHAPS VALUE THAT VARIABLE OF STORIES  UNDERWATER 

TO WORK THIS DIGNITY AND EGO STORY ROUTE WITH LIFE

 

IN STORIES OF THAT TOPIC OF ISSUE WONDERS TO NOTE WORK WITH STORIES OF TUBE VALUE PATH WITH THE STORY

OF TOPIC OF THE SIZEMIC ENERGY EFFECTED BY CRYOGENIC MACHINE OF EFFECT PATH OF NUCLEAR STORIES ROUTE WITH

STORIES IN TOPIC OF STORIES THAT PRESSURE EFFECT SPACE WORKING

ELECTRON WITH PROTON STORY OF PATH BASHING PROTONS ISSUE EFFECT WEATHER DOUBLES STORY WITH PATH NOTES

ROUTE OF TOPIC TO WORK THAT STORY ROUTE WITH PATH OF NOTES IN NOT DO BASHING PROTONS ROUTE WITH NOTES

HOWEVER ADD ELECTRON AND WORK WITH TOPICS NOTES STORIES NOTE ROUTE WITH THAT PATH OF ROUTE NOTES

 

NOTE ISSUE STORIES OF LIFE WITH ATTACKS DOUBLE MIMIC AND STORIES OF PATH WITH WHITE LIGHT GAP STORIES

ISSUE CONCERNS ROUTE WITH NOTES STORIES

 

ALSO CONCERNS WITH STORIES TO PATH NOTE ROUTE OF ISSUE PATH PERHAPS WHY WE ARE IN BAKING SODA OPIATES

AND BAKING SODA COCA ROUTE WITH STORIES

 

TOPICS ALSO ROUTE WITH STORIES

OF ISSUE ROUTE TO NOTES STORIES NOTES

 

STORIES OF ATTACK STORIES OF ROUTE TOPICS OF EXTRA PLANE IN LIFE STORIES TOPICS TO 911 SIMULATED GIANT BODY

ROUTE WITH PATH STORIES OF PATH STICKY PATH WITH ROUTE OF MEDS STORY NOTES TOPICS ALSO STORIES NOTES

 

TO STORIES ROUTE WITH  NOTES

 

PAST TO NOTES — — — — — — — - XXXXXXXXXXXXXXXXXXXXXXX IMPROVE THE ISSUE OF RELATIONSHIP OF NOTE 5 ANTENNA VIBE TO NOTES SOUND IS A PATH OF PRESSURE TO LIGHT ACTUALLY VIBE TO NOTES MAKE THE METAL OUT OF THE HYDROGEN SULFIDE TO NOTES LIGHTENING WENT TO GREEN NOTES VIBE EVENT TO NOTES NOT EVEN DOWN THE ROD VIBE TO NOTES https://www.youtube.com/watch?v=td0WEtf1pQk XXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXXX It was evident that calcium hydroxide increased recruitment, migration, proliferation, and mineralization of the DPSCs and periodontal ligament stem cells. pubmed.ncbi.nlm.nih.gov/20055661/ Dental stem cell therapy with calcium hydroxide in dental … HYDROXIDE EFFECT ON STEM CELLS

 

TOPIC OF MOOD MAKES US DIFFERENT TO HISTORY METHODIC TREE CLIMB TAKEN ROUTE WITH STORIES OF LIFE WITH ISSUE A TOPIC OF FLURRY BODY OF ROUTE 2 DIRECTION AND ANY DIRECTION STORIES ROUTE WITH ISSUE TO RELATE TO CHOICE OF DIRECTION STORY OF TOPIC ISSUE

STORY OF FLURRY ROUTE WITH 2 DIRECTION OF BODY DREAM ROUTE WITH LIFE STORIES TO ANY DIRECTION AND STORIES

OF PERSPECT SELF TO ANY DIRECTION AND STORY OF ISSUE THAT STORY IN FLURRY TO BODY ROUTE WITH ALSO

100 000 YEARS DREAMS OF STORY OF POLE TO TUBE STORY ROUTE WITH PATH TOPICS OF ISSUE TO NOTE BIKE PUMP STORIES

ROUTE WITH TRIANGLE 3D SHAPE ROUTE PREFIX SUFFIX ISSUES OF DREAM OF STORIES OF TOPIC PATH NOTES OF THAT STORY ROUTE WITH NOTES

STORY OF ISSUE ROUTE TO NOTES

 

MANY EVENT OF UPRIGHT METAL ATTACKS STORY HISTORY AND MEMORY BODY STORIES ARE 2 GENERAL ISSUE ON THE ATTACK SIDE STORIES

OF A NUMBER ISSUE TOPIC BOTHER GETTING INTO NUMBER TOPIC CONCERNS NOW STORIES WORKING THROUGH THIS TARGET

STORY NOTES ISSUE OF 2 ISSUE NOTES STORIES NOTES ALSO NOTES

 

 

FLOW OF SOLVENTS IN LIFE PRICE OF TOOL IN LIFE STORY OF VALUE OF LIFE TO STORY OF ISSUE TO NOTES PATH OF A MED IN LIFE

ISSUE IN LIFE TO STORY WONDERS ADD COIL TO SOLAR POWER IN LIFE STORY WITH ROUTE REJUVINATE MURITIC ACID VIBE

STORY AND RUN THE STORY OF SULFITES OF MEDS BACKWARDS THEN BULK AND THEN DRIP STORY VIBE TO NOTE ISSUES

ISSUE VIBE TO SULFIDE TO FLORIDE IONIC PATH TO NOTE DIRT WITH BACKWARS MURITIC ACID VIBE STORY WITH TO NOTE THEN TO DIETHYL ETHER

 


Oct 1, 2018 · Attempts to selectively oxidize mustard gas [(ClCH 2 CH 2) 2 S, abbreviated as BCES] to the non-toxic sulfoxide using a trans-Ru(TMP)(O) 2 /O 2 catalyst (TMP = porphyrin dianion of 5,10,15,20-tetramesitylporphyrin) have led to isolation and characterization, including an X-ray structure, of trans-Ru(TMP)(BCES) 2, the first such report of a ...

 

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During our studies on the oxidation of thioethers to sulfoxides [1], [2], [4], we were contacted by the Canadian Department of Defence, and received contract grants to investigate whether such chemistry was applicable to ‘Mustard Gas’ [bis(β-chloroethyl) sulfide, abbreviated as BCES]; this is a treacle-like liquid, whose vapour is toxic. The key factor is that the sulfoxide (ClCH2CH2)2SO is crystalline and as such is essentially non-toxic, while further oxidation generates the vesicant toxic sulphone [8]. Our studies ended in 1993, and reviews and new studies on reactivity of BCES, the simulant 2-chloroethyl(ethyl)sulfide (CEES), and other models, continue to appear [9], [10]; metal-organic framework systems are becoming increasingly involved [10](a), [10](b), and include studies on catalyzed selective oxidations to the sulfoxides [10b].
The thioethers Et2S and CEES, thiodiglycol, SOCl2, acetone, acetonitrile, and other common chemicals (all Aldrich products), and the deuterated solvents acetone-d6 and C6D6 (from MSD Isotopes), were used as received. The Ru source was obtained on loan from Johnson, Matthey Ltd. as RuCl3·3H2O (∼40% Ru), and the H2(TMP) and H2(OCP) porphyrins were kindly provided by D. Dolphin of this department.
1H and 13C{H} NMR spectra were measured on a Varian XL-300 or a Bruker AC200F spectrometer, with
Results and discussion
BCES (Mustard) was synthesized in small amounts by the reaction shown in Eq. (1), and is of high purity based on 1H and 13C{1H} NMR data. Only one previous publication in 1988 has reported 1H data, the δ values being given as 3.68 (Cl-CH2) and 2.92 (CH2-S) for the neat compound in the absence of solvent [17]: the multiplicities were not noted but our triplets measured in acetone-d6 (Table 1) are in excellent agreement and, as expected, are significantly downfield (∼2.5 ppm) from the CH3 triplet